Typical G.C. analysis

Perflavory

Typical G.C. analysis
#	%	Leftshift	Components
cistus oil
6	0.1		acetophenone
141	0.2	6-	acetoxy-11-nor-drim-7-en-9-one
72	0.2	7-	acetyl-2,2,6-trimethyl bicyclo(4.2.0)octane
119	0.1	6-	acetyl-5,8,8-trimethyl bicyclo(3.2.1)octan-2,3-dione
149	0.2	13-nor-	ambreinolide
148	0.1	8-epi-13-nor-	ambreinolide
78	0.2	alpha-	ambrinol
137	1.4		ambrox
144	0.1	6-oxo-iso	ambrox
81	0.9		aromadendr-1-ene
135	0.3		aromadendr-1(10)-en-9-one
91	1.4	1,5-(Z)-	aromadendr-9-ene
132	0.1	1,10-seco-	aromadendran-1,10-dione
130	0.1	5-epi-1,10-seco-	aromadendran-1,10-dione
86	1.5	allo-	aromadendrene
b3	0.4		benzoic acid
27	2.0		borneol
55	1.7		bornyl acetate
b21	0.9	3-iso	butenyl-5-methyl-5-vinyl butyrolactone
126	0.5		cadalene
98	0.4	delta-	cadinene
125	0.6	alpha-	cadinol
100	0.6	alpha-	calacorene
99	0.6	(E)-	calamenene
90	0.5	(Z)-	calamenene
b9	1.4	gamma-	campholenic acid
15	0.3	alpha-	campholenic aldehyde
10	0.3	gamma-	campholenic aldehyde
b7	0.3	alpha-	campholytic acid
b4	0.2	gamma-	campholytic acid
b5	2.4		camphonanic acid
b12	2.1	alpha-	camphoneic acid
18	0.1		camphor
60	0.8		carvacrol
48	0.2		carvenone
41	0.2	trans-	carveol
43	0.1	cis-	carveol
46	0.5		carvone
138	0.1	sesqui	chamaenol
117	1.8		copaborneol
127	0.6		copabornyl acetate
74	1.1	alpha-	copaene
82	0.7		cubeb-11-ene
113	4.1		cubeban-11-ol
121	0.4	1-epi-	cubenol
44	0.1		cuminaldehyde
b11	1.0	beta-	cyclogeranic acid
b8	0.9	gamma-	cyclogeranic acid
53	0.3	para-	cymen-7-ol
3	0.4	para-	cymene
b13	0.7		davanic acid
39	0.2		decanal
b20	3.8		decanoic acid
106	0.2	1,2-	dehydroglobulol
118	0.3	3,4-	dehydroglobulol
110	0.2	1-epi-3,4-	dehydroviridiflorol
104	1.4	1,2-	dehydroviridiflorol
146	0.2	14,15-	di-nor-8,13-epoxylabd-12-ene
79	0.1		dihydro-beta-ionene
94	0.2		dihydroactinidiolide
37	0.5	neo	dihydrocarveol
b15	6.5		dihydrocinnamic acid
b24	1.7		dimethyl (Z)-2-hexyl-3-methyl butendioic acid
49	0.2	2,4-	dimethyl acetophenone
9	1.0	alpha-para-	dimethyl styrene
97	0.2	4,7-	dimethyl tetral-1-one
b14	1.2	2,6-	dimethyl-5-oxoheptanoic acid
77	0.2		dodecanal
70	0.1	11-nor-	drim-7-ene
139	0.1		drim-8-en-7-one
69	0.2	11-nor-	drim-8-ene
101	0.3	11-nor-	driman-8-ol
102	0.2	beta-	elemol
35	1.3		elsholtzia ketone
136	0.2	5,11-	epoxycadin-1(10)-en-9-ol
108	0.8	5,11-	epoxycadin-1(10)-ene
8	0.8	6,8-	epoxymenth-1-ene
64	0.1		ethyl dihydrocinnamate
124	0.4	beta-	eudesmol
122	0.2	gamma-	eudesmol
65	1.6		eugenol
45	0.2	alpha-	fenchyl acetate
76	0.1	1-(	fur-2-yl methyl)-2-formyl pyrrole
b19	2.4		geranic acid
51	0.2		geraniol
80	0.1		geranyl acetone
109	0.5		gleenol
111	0.2		globulol
b2	0.5		heptanoic acid
b1	0.7		hexanoic acid
133	0.1	(Z)-3-	hexen-1-yl dihydrocinnamate
134	0.3		hexyl dihydrocinnamate
59	0.1	(2E,4E)-6-	hydroxy-2,6-dimethyl hepta-2,4-dienal
32	trace	2-	hydroxy-3-methyl benzaldehyde
66	0.2	2-	hydroxy-4-isopropenyl toluene
68	0.2	(E)-5-	hydroxy-para-mentha-1(6),8-dien-2-one
71	0.3	(Z)-5-	hydroxy-para-mentha-1(6),8-dien-2-one
140	0.1	10-	hydroxycalamene-8,9-epoxide
131	0.1	9-	hydroxyladanifer-10-one(9(10(1))-abeo-9-hydroxyaromadendran-10-one)
50	0.4	2-	hydroxypinan-3-one
87	0.2	(E)-beta-	ionone
142	0.6	15-nor-	labd-1(17)-ene
153	0.4		labd-7-en-15-ol
145	0.5	15-nor-	labd-7-ene
b31	6.3		labd-7-enoic acid
154	0.3		labd-8-en-15-ol
143	0.5	15-nor-	labd-8-ene
b32	4.0		labd-8-enoic acid
152	0.4		labd-8(17)-en-15-ol
b30	5.1		labd-8(17)-enoic acid
147	0.7	15-nor-	labdan-8-ol
b23	2.5		lauric acid
92	9.3		ledene
73	0.2	iso	ledene
116	1.3		ledol
12	0.2		linalool
7	0.4	(E)-	linalool oxide furanoid
11	0.2	(Z)-	linalool oxide furanoid
b28	1.0		linoleic acid
150	0.3		manoyl oxide
151	0.3	13-epi-	manoyl oxide
85	0.1		massoia lactone
40	0.3	(Z)-para-	menth-4(8)-en-2-ol
62	0.1	2-	methoxy-6-methyl acetophenone
29	0.3	para-	methyl acetophenone
52	1.0		methyl dihydrocinnamate
75	0.4		methyl eugenol
1	0.2	5-	methyl furfural
2	0.1	6-	methyl-5-hepten-2-one
120	0.3		muurola-4,10(14)-dien-1-ol
123	0.3	alpha-	muurolol
b25	2.7		myristic acid
33	0.9		myrtenal
b18	6.0		myrtenic acid
36	1.5		myrtenol
58	1.1		naginata ketone
22	0.2		nerol oxide
103	0.2	(E)-	nerolidol
13	0.1		nonanal
b10	1.6		nonanoic acid
17	0.7	(E)-3-	nonen-2-one
b6	3.7		octanoic acid
b27	1.2		oleic acid
115	0.1	beta-	oplopenone
b26	5.1		palmitic acid
105	1.2		palustrol
129	0.1		pentadecanal
42	0.1	3-	phenyl propanol
23	1.5		pinocamphone
28	0.7	iso	pinocamphone
19	1.8	trans-	pinocarveol
24	0.3		pinocarvone
63	0.4	trans-	pinocarvyl acetate
47	0.8		piperitone
25	0.1		propiophenone
128	0.2	4-iso	propyl-6-methyl tetral-1-one
16	0.1	(E)-	rose oxide
14	0.2	(Z)-	rose oxide
20	0.1	(E)-	sabinol
b29	0.8		stearic acid
21	0.2	(E)-	tagetone
26	0.2	(Z)-	tagetone
31	0.8		terpinen-4-ol
34	0.5	alpha-	terpineol
114	0.1		tetradecanal
89	0.6	1,1,5,6-	tetramethyl-1,2-dihydronaphthalene
95	0.2	1,1,5,6-	tetramethyl-1,2,3,4-tetrahydronaphthalene
54	0.2		thymol
107	0.2	6-para-	tolyl heptan-2-one
88	0.1		tridecanal
b16	0.7	1,5,5-	trimethyl bicyclo(4.1.0)heptan-7-carboxylic acid A
b17	1.9	1,5,5-	trimethyl bicyclo(4.1.0)heptan-7-carboxylic acid B
5	0.3	2,2,6-	trimethyl cyclohex-2-enone
4	1.3	2,2,6-	trimethyl cyclohexanone
93	0.2	1-(1,2,2-	trimethyl cyclopent-1-yl) pentan-1,4-dione
96	0.2	6,6,10-	trimethyl decan-2-one
30	0.5	2,2,5-	trimethyl oxepan-4-one
67	0.2	1,1,6-	trimethyl-1,2-dihydronaphthalene
83	0.1	4,4,7a-	trimethyl-1,4,5,6,7,7a-hexahydro-2H-inden-2-one
84	0.1		tuberolactone
61	0.2		undecanal
b22	0.3		undecanoic acid
38	0.3		verbenone
112	4.3		viridiflorol
56	0.2		vitispirane A
57	0.1		vitispirane B
P. Weyerstahl, H. Marschall, M. Weirauch, K. Thefeld and H. Surburg, Constituents of commercial labdanum oil. Flav. Fragr. J., 13, 295-318 (1998). P&F 24, No. 4, 31, (1999)
tagetes minuta flower oil CO2 extract
#	%	Leftshift	Components
54	3.56		alchenenotriol
30	9.98	(E)-	anethole
27	2.10	para-	anisaldehyde
41	0.33		aromadendrene
47	0.08	beta-	bisabolene
48	0.12	gamma-	cadinene
14	0.11		camphor
24	0.23	cis-	carveol
40	3.44	beta-	caryophyllene
23	0.61		citronellol
2	1.12	para-	cymene
31	1.51		dehydroelshotzia ketone
20	0.12	(Z)-	dihydrocarvone
6	5.19		dihydrotagetone
9	0.22	alpha-para-	dimethyl styrene
33	3.00	delta-	elemene
50	0.11	gamma-	elemene (furanoid)
21	0.15		elsholtzia ketone
49	0.15		eugenyl acetate
37	0.28		geranyl acetate
53	0.28		guaiol
42	2.14	alpha-	humulene
51	0.29		ledol
3	15.14		limonene
11	1.03		linalool
8	0.43	(Z)-	linalool oxide furanoid
28	0.47		linalyl acetate
10	0.12	(E)-para-	menth-2-en-1-ol
29	0.39		methyl citronellate
39	0.24		methyl eugenol
43	0.22	6-	methyl-gamma-ionone
45	0.29	alpha-	muurolene
1	0.24		myrcene
34	0.19		neryl acetate
5	0.30	(E)-beta-	ocimene
4	19.33	(Z)-beta-	ocimene
36	0.10	beta-	patchoulene
46	0.13		pentadecane
17	0.30	(Z)-	pinanone
13	3.68	(Z)-	sabinene hydrate
35	0.32	(E)-iso	safrole
52	2.42		spathulenol
26	0.65	(E)-	tagetenone
25	13.26	(Z)-	tagetenone
15	2.81	(E)-	tagetone
16	0.34	(Z)-	tagetone
18	0.46		terpinen-4-ol
7	0.26	gamma-	terpinene
19	0.50	alpha-	terpineol
38	0.16		tetradecane
12	0.24	alpha-	thujone
32	0.12		tridecane
44	0.57		valencene
22	0.05		verbenone
J. Daghero, M. Mattea, E. Reverchon, G. Della Porta and F. Senatore, Isolation of Tagetes minuta L. oil using supercritical CO2 extraction. In: Proceedings WOCMAP-2. Edits., V. Martino, A. Bandoni, G. Bleak and N. Capelle, Acta Hort., 503, 21-25 (1999). P&F 25, No. 6, 32, (2000)

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