Perflavory
Typical G.C. analysis
cinnamomum zeylanicum bark oil india
In 1989, Variyar and Bandyopadhayay used retention time data of authentic compounds on a packed GC column to determine the composition of bark and twig oils of Cinnamomum zeylanicum of Kerala (India) origin. The compounds characterized in these oils can be seen in Table VIII. Only the bark oil will be shown here:
#%LeftshiftComponents
50.90beta- caryophyllene
30.261,8- cineole
882.11(E)- cinnamaldehyde
100.95(E)- cinnamyl acetate
97.69(E)- cinnamyl alcohol
110.41  coumarin
120.76  eugenol
70.28alpha- humulene
20.18  limonene
42.48  linalool
10.18alpha- pinene
60.80  terpinen-4-ol

P. S. Variyar and Bandyopadhayay, On some chemical aspects of Cinnamomum zeylanicum. PAFAI, (Oct/Dec), 35-38 (1989).

P&F 23, No. 1, 39, (1998)

cinnamomum zeylanicum bark oil sri lauka
Using GC (retention indices) Bouzid et al. (1997) analyzed an oil of cinnamon bark. The compounds identified were as follows:
#%LeftshiftComponents
11trace-0.05  benzaldehyde
250.40-1.00  benzyl benzoate
20.04-0.05  camphene
40.01-0.02delta-3- carene
19trace-0.12  caryophyllene
131.00-2.00beta- caryophyllene
2072.00-82.15(E)- cinnamaldehyde
170.12-0.98(Z)- cinnamaldehyde
213.24-3.65(E)- cinnamyl acetate
230.50-0.60(E)- cinnamyl alcohol
100.04-0.05alpha- copaene
90.25-0.35para- cymene
221.07-13.30  eugenol
140.20-0.62alpha- humulene
70.09-0.10  limonene
120.70-1.06  linalool
50.06para-menthene
180.09-0.15ortho- methoxybenzaldehyde
240.30-0.80ortho- methoxycinnamaldehyde
60.07-0.08  myrcene
80.40-0.64beta- phellandrene
160.10-0.70  phenyl propionaldehyde
10.04-0.07alpha- pinene
30.02-0.03beta- pinene
150.35-0.62alpha-terpineol + borneol
cinnamomum zeylanicum fruit oil india
In 1997, Jayaprakasha et al. analyzed two oils of the fruit of C. zeylanicum by GC and GC/MS. Although the oils were produced from fruit harvested in two different locations in India, Karnataka and Kerala, the oil compositions were similar as can be seen from the following analytical results:
#%LeftshiftComponents
322.7-2.8  benzyl benzoate
80.3-0.4  borneol
212.3-3.0delta- cadinene
201.2-1.6gamma- cadinene
311.0-1.5alpha- cadinol
302.7-3.4T- cadinol
159.2-13.7beta- caryophyllene
240.9-1.1  caryophyllene oxide
100.6-4.3(E)- cinnamaldehyde
70.2-0.3(Z)- cinnamaldehyde
1642.4-54.2(E)- cinnamyl acetate
112.0-2.2(E)- cinnamyl alcohol
141.8-3.1alpha- copaene
290.5-0.8  cubenol
270.4-0.510-epi-gamma- eudesmol
120.2-0.3  eugenol
191.7-2.0  germacrene B
180.7-0.8  germacrene D
260.3  germacrene D-4-ol
250.5-0.6  globulol
220.4beta- guaiene
172.8-3.1alpha- humulene
340.0-0.3  methyl oleate
330.0-0.3  methyl palmitate
280.3alpha- muurolol
30.0-0.2  myrcene
230.2-0.4  nerolidol
60.2-0.5(E)-beta- ocimene
40.1-0.7alpha- phellandrene
50.4-1.6beta- phellandrene
132.9-4.33- phenyl propyl acetate
10.1-1.6alpha- pinene
20.1-0.6beta- pinene
90.3alpha- terpineol

G. K. Jayaprakasha, L. Jaganmohan Rao and K. K. Sakariah, Chemical composition of the folatile oil from the fruits of Cinnamomum zeylanicum Blume. Flav. Fragr. J., 12, 331-333 (1997)

P&F 23, No. 1, 39, (1998)

cinnamomum zeylanicum twig oil india
In 1989, Variyar and Bandyopadhayay used retention time data of authentic compounds on a packed GC column to determine the composition of bark and twig oils of Cinnamomum zeylanicum of Kerala (India) origin. The compounds characterized in these oils can be seen in Table VIII. Only the twig oil will be shown here:
#%LeftshiftComponents
50.73beta- caryophyllene
30.641,8- cineole
876.07(E)- cinnamaldehyde
100.43(E)- cinnamyl acetate
99.55(E)- cinnamyl alcohol
110.32  coumarin
124.03  eugenol
70.19alpha- humulene
20.14  limonene
43.05  linalool
10.21alpha- pinene
60.50  terpinen-4-ol

P. S. Variyar and Bandyopadhayay, On some chemical aspects of Cinnamomum zeylanicum. PAFAI, (Oct/Dec), 35-38 (1989).

P&F 23, No. 1, 39, (1998)

hyacinthus orientalis absolute
#%LeftshiftComponents
340.21-0.27  benzaldehyde
4736..84-44.24  benzyl acetate
521.78-1.95  benzyl alcohol
732.94-3.06  benzyl benzoate
630.80-0.13  benzyl tiglate
33trace2-sec- butyl-3-methoxypyrazine
35trace2-iso butyl-3-methoxypyrazine
20.01-0.05  camphene
390.02beta- caryophyllene
110.011,8- cineole
59trace  cinnamaldehyde
650.21-0.32  cinnamyl acetate
703.46-4.04(E)- cinnamyl alcohol
67trace(Z)- cinnamyl alcohol
560.02-0.04  creosol
170.05-0.56para- cymene
320.01-0.02  decanal
680.29-0.32  elemicin
440.05-0.09  ethyl benzoate
661.57-1.68  eugenol
420.00-trace(E)-beta- farnesene
46trace-0.03(Z,E)-alpha- farnesene
30.02  hexanal
230.03-0.04  hexanol
250.76-2.66(Z)-3- hexen-1-ol
280.02(E)-2- hexen-1-ol
240.03-0.08(E)-3- hexen-1-ol
210.02-0.05(Z)-3- hexen-1-yl acetate
64trace(Z)-3- hexen-1-yl benzoate
310.00-0.01(Z)-3- hexen-1-yl butyrate
150.04-0.19(Z)-3- hexen-1-yl formate
430.32-0.48(Z)-3- hexen-1-yl tiglate
16trace-0.01  hexyl acetate
483.80-3.94 hydroquinone dimethyl ether + (E,E)-alpha-farnesene
720.05-0.08  indole
90.53-1.00  limonene
360.03  linalool
710.00-trace2-(4- methoxyphenyl) ethyl alcohol
40.012- methyl (E)-2-butenal
600.01-0.10  methyl 2-methoxybenzoate
270.01-0.024- methyl anisole
690.02-0.03  methyl anthranilate
400.09-0.10  methyl benzoate
571.12-1.40  methyl eugenol
62trace  methyl N-methyl anthranilate
490.04-0.07  methyl salicylate
220.01-0.036- methyl-5-hepten-2-one
71.80-2.05  myrcene
260.01-0.03  nonanal
1313.72-14.93(E)-beta- ocimene
120.75-1.01(Z)-beta- ocimene
190.02-0.05  octanal
370.04  octanol
140.02-0.033- octanone
300.66-1.301- octen-3-ol
200.011- octen-3-one
60.01-0.021- penten-3-ol
8trace-0.01alpha- phellandrene
100.01beta- phellandrene
511.62-2.482- phenethyl acetate
538.96-16.392- phenethyl alcohol
740.40-0.532- phenethyl benzoate
50trace2- phenethyl formate
410.02-0.05  phenyl acetaldehyde
550.05-0.063- phenyl propyl acetate
580.81-0.863- phenyl propyl alcohol
10.08-0.16alpha- picoline
50.05-0.06gamma-picoline
29trace2-iso propyl-3-methoxypyrazine
450.00-0.04alpha- terpineol
180.01  terpinolene
611.12-1.261,2,4- trimethoxybenzene
380.16-0.172- undecanone
E. J. Brunke, F. J. Hammerschmidt and G. Schmaus, Head-space analysis of hyacinth flowers Fla.. Fragr J., 9, 56-69 (1994). P&F 20, No. 6, 35, (1995)
narcissus absolute
#%LeftshiftComponents
99.58  benzyl acetate
114.79  benzyl alcohol
164.00  benzyl benzoate
26.57delta-3- carene
41.461,8- cineole
152.87(E)- cinnamyl alcohol
61.27para- cymene
130.53(E)- ethyl cinnamate
32.15  limonene
70.62  linalool
140.19  methyl anthranilate
1215.84(E)- methyl cinnamate
100.51  nerol
12.39alpha- pinene
527.21gamma- terpinene
80.33alpha- terpineol

S. Bruno, N. de Laurentis, A. Amico and L. Stefanizzi, Chemical investigation and cytologic localization of essential oils in the flowers of Narcissus tazetta. Int. J. Pharmacog., 32, 357-361 (1994).

P&F 22, No. 2, 59, (1997)

narcissus tazetta ssp. tazzetta absolute
#%LeftshiftComponents
99.53  benzyl acetate
101.70  benzyl alcohol
160.65  benzyl benzoate
28.40delta-3- carene
43.031,8- cineole
140.81(E)- cinnamyl alcohol
68.53para- cymene
125.63(E)- ethyl cinnamate
151.51  indole
33.25  limonene
711.70  linalool
130.43  methyl anthranilate
111.13(E)- methyl cinnamate
16.07alpha- pinene
510.29gamma- terpinene
81.95alpha- terpineol

S. Bruno, N. de Laurentis, A. Amico and L. Stefanizzi, Chemical investigation and cytologic localization of essential oils in the flowers of Narcissus tazetta. Int. J. Pharmacog., 32, 357-361 (1994).

P&F 22, No. 2, 59, (1997)

ylang ylang flower oil
#%LeftshiftComponents
510.13alpha- amorphene
290.35(E)- anethole
50.94  benzaldehyde
2011.63  benzyl acetate
112.20  benzyl alcohol
636.19  benzyl benzoate
330.04  benzyl butyrate
651.37  benzyl salicylate
580.07alpha- bisabolol
470.713- buten-2-yl benzoate
360.08  butyl benzoate
530.16delta- cadinene
540.12gamma- cadinene
600.12 cadinol
610.12alpha- cadinol
421.69beta- caryophyllene
570.07  caryophyllene oxide
120.091,8- cineole
432.09(E)- cinnamyl acetate
300.26(E)- cinnamyl alcohol
380.13alpha- copaene
170.09para- cresol
100.34para- cresyl methyl ether
450.58beta- cubebene
260.131,4- dimethoxybenzene
250.173,4- dimethoxytoluene
211.46  ethyl benzoate
440.37(Z)-iso eugenol
522.34(E,E)-alpha- farnesene
620.84(E,E)- farnesol
640.61(E,E)- farnesyl acetate
371.96  geranyl acetate
495.55  germacrene D
30.28(E)-2- hexen-1-ol
90.16(Z)-3- hexen-1-yl acetate
550.19(Z)-3- hexen-1-yl benzoate
460.74alpha- humulene
130.07  limonene
1835.49  linalool
220.072- methoxy-4-methyl phenol
150.172- methoxyphenol
390.114-methoxyphenyl methyl acetate
310.05  methyl 2-methoxybenzoate
350.06  methyl 4-methoxybenzoate
320.08  methyl anthranilate
166.50  methyl benzoate
480.86  methyl eugenol
230.29  methyl salicylate
20.063- methyl-2-butenol
40.333- methyl-2-butenyl acetate
10.072- methyl-3-butenol
500.14gamma- muurolene
590.11alpha- muurolol
80.16  myrcene
270.27  nerol
560.13(E)- nerolidol
140.14(E)-beta- ocimene
280.202- phenyl-1-nitroethane
61.87alpha- pinene
70.66beta- pinene
340.084-(2- propenyl) phenol
240.14alpha- terpineol
415.51  tetradecane
400.16alpha- ylangene

E. E. Stashenko, W. Torres and J. R. Martinez Morales, A study of the compositional variation of the essential oil of ylang ylang (Cananga odorata Hook. fil. et Thomson, forma genuina) during flower development. J. High Resol. Chromatogr., 18, 101-104 (1995).

P&F 24, No. 4, 31, (1999)
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